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Wet Bench Solvent, wbsolvent

The Solvent Wet Bench is used for manual solvent cleaning of silicon wafers, tweezers, glassware, or any other inert objects such as equipment parts. The bench is equipped with a carboy to collect solvent waste , two hot plates for heating solvents in beakers, an ultrasonic bath, and a N2 gun for drying.

Picture and Location

 Wet Bench Solvent

The tool is located at C4 on the Lab Map.

Process Capabilities

Cleanliness Standard

 The wbsolvent appears in all three equipment groups (clean, semiclean, and gold).

Performance of the Tool

What the Tool CAN do

  • The wbsolvent wet bench is for solvent processing of standard and non-standard materials. Such materials include wafer pieces or substrates with gold or other non-standard films. All processing is done manually in station-dedicated or labuser-provided labware (beakers, dishes, etc.). Any labware provided at the wbsolvent station is considered gold-contaminated.
  • Substrates may be of most any type, size, shape and any material, subject to the constraints in the Materials Allowed section. GaAs is allowed for processing in labuser-provided labware.
  • SNF standard solvents (consult the Materials List on the SNF website for acceptable chemicals) are allowed at this bench, for standard processing only. Consult staff if your work requires non-standard processing conditions (such as elevated temperatures, unusually extended process times, or mixing of chemicals), even if standard SNF solvents are to be used.

 

What the Tool CANNOT do

  • There are no automated wafer processing modules at this station.

 

How to Become a User

 

  1. Read all material on the SNF website concerning the wbsolvent.
  2. Contact SNF training contact on the Equipment Summary page.

 

Operating Procedures

 

System Overview

This is a stainless steel wet bench. This station contains (from left to right):
A carboy to collect solvents, two explosion proof hot plates in stainless steel wells with controllers mounted in the upper panel, an ultrasonic bath and a N2 gun.

Chemical Hazards

Only SOLVENTS (flammables) are to be used at this wetbench (no Chlorobenzene). You must be familiar with the Material Data Safety Sheets (MSDSs) of the chemicals you will be using and understand safe chemical handling procedures before working at this station. Acids or bases are not allowed.
Solvents commonly used at this bench are:
Isopropanol (IPA), Flash point: 12C (54F)
Acetone, Flash point: -20C (-4F)
Methanol, Flash point: 12C (54F)

In air, above a critical temperature, called the "flash point", the vapors from a flammable can ignite and explode. The source of ignition may be heat (such as a hot plate) or a spark (such as from an electrical tool). Because the vapors can travel over considerable distances, the source of ignition can be far away from the flammables container itself.
Always work well within the exhausted area of bench (behind the red line). The air pulled into the exhaust area will keep the concentration of vapors below the flash point. Where possible, minimize the quantities of flammables used. Before working with flammables, always note the location of the nearest safety shower and fire extinguisher. Flammables should be stored in the designated flammables cabinet; no flammables may be stored at the bench.

We are required by the Stanford University - Utilities Services (Environmental Quality and Water Efficiency) to distribute the Best Management Practices (BMP) fact sheet, you'll find the link here in the Stanford University - Utilities Services folder.
Please read the fact sheet and reduce the amount of pollutant for example by using smaller quantities of chemicals.

 

Equipment Hazards

Input power is 208 volts AC, three phase at 30 AMPS. Only qualified personnel are allowed to work on the electrical parts of this system. If any electrical problems are seen with this system, press the EMERGENCY POWER OFF button, shut the system down and contact Maintenance staff. Pressing the EMERGENCY POWER OFF button will shutdown the hotplates and the ultrasonic bath.
If the exhaust shuts down while there are solvents in the bench press the EMERGENCY POWER OFF button and EVACUATE THE LAB using one of the red pager phones.
Do not leave the bench unattended when you are using the hot plates. Be sure that the Hot Plates are turned off when not in use.
Do not leave the bench unattended when you are using the heated ultrasonic bath!

The only drain on the wetbench is to the solvent collection container (carboy). DO NOT WORK WITH ANYTHING OTHER THAN SOLVENTS AT THIS STATION -- If acids are poured down the drain A VIOLENT ACTION WILL OCCUR.

Process Hazards

General process hazards involve handling of chemicals and materials which come into contact with chemical used at this station. Wet benches are potentially the most dangerous operations in the lab. Be sure you understand all hazards and proper handling procedures before working at any wet bench.

Instructions

  1. Make sure the exhaust is working.
  2. Be aware of the location of the nearest safety shower and eyewash.
  3. Wear safety glasses or face shield and solvent resistant gloves.
  4. Check the bench for any damage or any other obvious problems. Notify Maintenance if any problems are observed.
  5. Users are allowed to make a reservation.
  6. Enable wbsolvent.
  7. Press the main power button (upper left on the control panel). If you are not using the hotplates, make sure the switches are off otherwise the hotplates start to heat!
  8. Only SOLVENTS may be used at this wetbench. Any of the SNF-approved solvents may be used at this bench. Any non-SNF-approved solvents must undergo safety and contamination review by the ProM Committee.
  9. Labware provided at this bench are mainly Pyrex glass beakers and labeled wbsolvent, your wafers will be "gold" contaminated. Please don't use labware from other benches. You are responsible for supplying your own labware if you are processing "clean" or "semiclean" wafers or GaAs wafers.
  10. Fill out a "IN-USE HAZARDOUS CHEMICALS" card for each open container.
  11. Transfer solvents from the flammable cabinets to this bench in a metal cart, never hand-carry chemicals.
  12.  Always open bottles under the exhausted area, about 6 inches under the hood, to prevent fumes from escaping into the room. Place the bottle cap upside down on a bench. Do not touch the inside of the bottle cap or the area around the mouth of the bottle with your gloves.
  13. There are two hot plates with controllers mounted in the upper panel. A setting of 2 or 3 should be sufficient for heating solvents at this bench. Always keep a thermometer inside of the beaker to control the heat.  Do not leave the hot plates on when you are finished using them.
  14. The bench has a heated ultrasonic bath that is to be used for ultrasonic cleaning of wafers (pieces to 4" wafers only). Fill the bath with DI water (from wet bench general) up to the liquid level line and place beaker with solvent inside the water bath. Fill out a "IN-USE HAZARDOUS CHEMICALS" card for the solvent. Be sure to drain the solvent into the carboy when you are through, turn off the ultrasonic generator, and turn off the heater to the ultrasonic when you are finished using it.
  15. Collect solvent contaminated solid waste like wipes, gloves or labware in a zip-lock bag, close the bag within the exhausted area and place the bag in a hazardous waste container in the photolithography area.

Shutdown

  1. Do not leave solvents at the wetbench. Solvents should be disposed of in the carboy. If acids are poured down the drain a violent action will occur. If the carboy is full, report it.
  2. Turn off the hotplates or ultrasonic bath.
  3. Be sure you are leaving the station in a neat condition. Do not leave wipes on the surface of the wetbench, they will be sucked to the back of the bench and get onto the hotplates.
  4. Disable wbsolvent.

 

Facilities

The facilities of the Santa Clara Plastics Solvent Wet Bench are as follows:

  exhsc-f16

Exhaust Scrubbed

 

hn2-f1
House Nitrogen

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